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Korean J. Met. Mater.
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Korean Journal of Metals and Materials
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Korean J. Met. Mater.
2024;62(4):299-305. Published online 2024 Mar 29
DOI:
https://doi.org/10.3365/KJMM.2024.62.4.299
Abstract
To improve the hydrogen-storage properties of Mg
2
Ni, LiBH
4
was added by milling in hydrogen atmosphere (reactive mechanical milling, RMM). Mg
2
Ni-10LiBH
4
was prepared with a composition of 90 wt% Mg
2
Ni + 10 wt% LiBH
4
. The quantity of released hydrogen (H
r
) versus temperature T curve for Mg
2
Ni10LiBH
4
was obtained by heating at.....
More
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친환경 Ti 및 TiH
2
분말 제조를 위한 TiO
2
의 칼슘열환원에 대한 기초연구
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박성훈, 강정신, 손호상
Korean J. Met. Mater.
2024;62(3):190-203. Published online 2024 Feb 28
DOI:
https://doi.org/10.3365/KJMM.2024.62.3.190
Abstract
To develop an eco-friendly titanium (Ti) production process, the calciothermic reduction of titanium dioxide (TiO
2
) was investigated. The mechanism involved in the reduction of TiO
2
using calcium (Ca) was examined. The influence of a molten salt, calcium chloride (CaCl
2
), on the calciothermic reduction was investigated by conducting experiments at 1123.....
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전기화학적 및 고압 수소 분위기하 템퍼드 마르텐사이트강의 수소취화 특성 비교
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김상규, 김재윤, 서현주, 정환교, 박재영, 백운봉, 황병철
Korean J. Met. Mater.
2023;61(11):807-814. Published online 2023 Oct 29
DOI:
https://doi.org/10.3365/KJMM.2023.61.11.807
Abstract
The effect of hydrogen charging methods on the hydrogen embrittlement characteristics of tempered martensitic steels were discussed in terms of hydrogen diffusion behavior. Two tempered martensitic steels with different Si content were fabricated by quenching and tempering. The steel with high Si content had a lower cementite fraction because the.....
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황 함량 변화가 NiZnS 복합광촉매의 태양광 물분해 효율에 미치는 영향
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김주현, 강은선, 김정현
Korean J. Met. Mater.
2023;61(4):284-290. Published online 2023 Mar 22
DOI:
https://doi.org/10.3365/KJMM.2023.61.4.284
Abstract
Solar energy is attracting much attention as an eco-friendly source for future energy needs. Herein, NiZnS photocatalysts were synthesized with a hydrothermal method at various sulfur contents. The ZnS material is widely used as a photocatalyst because of its high stability, low toxicity, and excellent charge separation characteristics. Nickel is.....
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자동차용 초고강도 강재의 전기아연도금 시 음극전류 인가조건이 수소 유입, 취화 및 부식유기 수소취화 거동에 미치는 영향
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방혜린, 박진성, 김상헌, 김태엽, 오민석, 김성진
Korean J. Met. Mater.
2023;61(3):145-156. Published online 2023 Feb 24
DOI:
https://doi.org/10.3365/KJMM.2023.61.3.145
Abstract
The effects of the electrogalvanizing conditions (a combination of plating current and time) on hydrogen infusion, embrittlement, and corrosion-induced hydrogen embrittlement (HE) behaviors of ultra-high strength steel were examined. A range of experimental and analytical methods, including electrochemical impedance spectroscopy, hydrogen permeation, polarization, and slow strain rate test, were employed......
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Web of Science 2
Crossref 1
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Korean J. Met. Mater.
2023;61(2):115-119. Published online 2023 Jan 27
DOI:
https://doi.org/10.3365/KJMM.2023.61.2.115
Abstract
As interest in hydrogen energy grows, eco-friendly methods of producing hydrogen are being explored. CuBi
2
O
4
is one of the p-type semiconductor cathode materials that can be used for photoelectrochemical hydrogen production via environment-friendly water electrolysis. CuBi
2
O
4
has a bandgap of 1.5 – 1.8 eV which allows it to photogenerate electrons.....
More
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소부경화강의 변형 시효 및 수소취성 거동에 미치는 미세조직의 영향
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김재윤, 고석우, 황병철
Korean J. Met. Mater.
2022;60(11):811-818. Published online 2022 Oct 31
DOI:
https://doi.org/10.3365/KJMM.2022.60.11.811
Abstract
The strain aging and hydrogen embrittlement behavior of two bake hardening (BH) steels with different microstructures were investigated in this study. The single-phase BH steel was composed of fully ferrite, while the dual-phase BH steel consisted of ferrite and 3 % martensite. The BH index and aging index (AI) of.....
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Web of Science 3
Crossref 3
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수소 저장용 다공성 제올라이트 탐색을 위한 고속 대량 스크리닝 계산
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여병철
Korean J. Met. Mater.
2022;60(7):537-544. Published online 2022 Jun 3
DOI:
https://doi.org/10.3365/KJMM.2022.60.7.537
Abstract
Hydrogen is considered an attractive energy resource because it is eco-friendly in contrast with fossil fuels. Hydrogen storage remains as essential technology for increasing the use of the hydrogen in applications such as hydrogen vehicles and fuel cells. Hydrogen storage requires retaining a high density of hydrogen molecules at ambient.....
More
Crossref 1
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Korean J. Met. Mater.
2022;60(3):180-187. Published online 2022 Feb 8
DOI:
https://doi.org/10.3365/KJMM.2022.60.3.180
Abstract
In this study, Ti-10Mo alloy powder and sintered bodies were successfully fabricated using a threestep process of acid/organic solvent cleaning, hydrogenation/dehydrogenation (HDH) of bulk Ti-Mo scrap, and pressureless vacuum sintering of the alloy powder. This process can be used to recycle valuable Ti alloy. And unlike remelting-based recycling processes, in.....
More
Web of Science 1
Crossref 3
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수소 분위기에서 Mg와 VCl
3
의 밀링에 의한 Mg의 수소 흡수 방출 특성의 향상
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송명엽, 이성호, 곽영준
Korean J. Met. Mater.
2021;59(10):709-717. Published online 2021 Sep 6
DOI:
https://doi.org/10.3365/KJMM.2021.59.10.709
Abstract
VCl
3
(vanadium (III) chloride) was selected as an additive to Mg to increase the hydrogenation and dehydrogenation rates and the hydrogen storage capacity of Mg. Instead of MgH
2
, Mg was used as a starting material since Mg is cheaper than MgH
2
. Samples with a composition of 95 wt% Mg +.....
More
Crossref 5
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미량의 H
2
S 함유 수용액 환경 내 CO
2
첨가가 고강도 철강소재의 부식 및 수소침투거동에 미치는 효과
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류승민, 박진성, 방혜린, 김성진
Korean J. Met. Mater.
2021;59(8):533-544. Published online 2021 Jul 5
DOI:
https://doi.org/10.3365/KJMM.2021.59.8.533
Abstract
The effects of adding CO
2
to low level H
2
S containing aqueous environment on the corrosion and hydrogen penetration behaviors of high-strength steel were evaluated using a range of experimental and analytical methods. The corrosion rate of the steel sample exposed to a low level of H
2
S dissolved in an aqueous.....
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Web of Science 3
Crossref 3
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초음파 분무 열분해법으로 제조한 텅스텐 미세분말의 미세조직과 소결 거동
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조현희, 김정현, 이영인, 정영근, 오승탁
Korean J. Met. Mater.
2021;59(5):289-294. Published online 2021 Apr 6
DOI:
https://doi.org/10.3365/KJMM.2021.59.5.289
Abstract
The powder microstructure and sintering behavior of W prepared by ultrasonic spray pyrolysis and spark plasma sintering were investigated. Fine-grained W powders were synthesized by ultrasonic spray pyrolysis using an ammonium metatungstate hydrate solution and hydrogen reduction. The XRD analysis of the powder, pyrolyzed below 600
o
C, showed tungsten oxide.....
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Web of Science 2
Crossref 2
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Korean J. Met. Mater.
2021;59(4):268-272. Published online 2021 Mar 24
DOI:
https://doi.org/10.3365/KJMM.2021.59.4.268
Abstract
Boron Nitride Nanotubes (BNNT) are one of the candidate materials for storing hydrogen by physical adsorption. It has been reported that this hydrogen storage capacity increases as the crystallinity of the nanostructures decreases. Here, BNNT was synthesized using an RF plasma torch system, and the surface of the BNNT was.....
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Web of Science 2
Crossref 2
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인장강도 600 MPa급 저탄소강 필렛 용접부의 저온균열과 미세조직에 따른 수소취성 민감성 및 수소확산 거동
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안형진, 이정훈, 박한지, 유재석, 정성욱, 박종민, 강남현
Korean J. Met. Mater.
2021;59(1):21-32. Published online 2021 Jan 5
DOI:
https://doi.org/10.3365/KJMM.2021.59.1.21
Abstract
Hydrogen flowing into a weld causes hydrogen embrittlement (HE), so to prevent cold cracks in the weld, HE must be suppressed. In this study, single-pass fillet weldments were fabricated using two different welding fillers with the same strength level as the American Welding Society standard. The specimen F-HNi, which had.....
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Web of Science 8
Crossref 7
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구리함량 변화에 따른 Cu
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S 광촉매 제조 및 태양광 물분해 수소 생산 특성 연구
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강수진, 김정현
Korean J. Met. Mater.
2020;58(12):907-914. Published online 2020 Dec 4
DOI:
https://doi.org/10.3365/KJMM.2020.58.12.907
Abstract
Solar water splitting is an attractive method for producing hydrogen from renewable natural resources, and heterostructure photocatalysts have been widely investigated for photocatalytic applications. Hetero-component photocatalysts can reduce the charge recombination process by improving electron utilization, and are considered promising candidates for solar water splitting. Amongst various heterostructure systems, combinations.....
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Web of Science 5
Crossref 4
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페라이트-펄라이트 조직 저탄소강의 수소 취성에 미치는 Nb 첨가와 예비 변형의 영향
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고석우, 이지민, 황병철
Korean J. Met. Mater.
2020;58(11):752-758. Published online 2020 Oct 15
DOI:
https://doi.org/10.3365/KJMM.2020.58.11.752
Abstract
The effect of pre-strain on the hydrogen embrittlement of Nb-free and Nb-added low-carbon steels with ferrite-pearlite structure was investigated in this study. After the steels were electrochemically charged with hydrogen, slow-strain rate tensile (SSRT) tests were conducted on them to examine hydrogen embrittlement behavior. The SSRT test results revealed that.....
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Web of Science 4
Crossref 4
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수소가압 및 응력부식 분위기에서 스테인레스강 SS304의 수소취성균열
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최병학, 이상우, 안종기, 이진희, 임태운
Korean J. Met. Mater.
2020;58(10):653-659. Published online 2020 Oct 5
DOI:
https://doi.org/10.3365/KJMM.2020.58.10.653
Abstract
The phenomena of hydrogen induced cracking (HIC) in 304 stainless steels was considered in a hydrogen pressure and stress corrosive atmosphere. Microstructures with chloride pits and stress corrosion cracks around the HIC were analyzed by SEM/EDS. Abnormal phase transformations induced by the hydrogen were analyzed using TEM and diffraction. In.....
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Web of Science 5
Crossref 4
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A516-65급 압력용기용 강재의 용접모사 열처리를 통한 용접열영향부의 수소확산 및 황화물응력균열 거동 연구
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조동민, 박진성, 이진우, 김성진
Korean J. Met. Mater.
2020;58(9):599-609. Published online 2020 Aug 13
DOI:
https://doi.org/10.3365/KJMM.2020.58.9.599
Abstract
Hydrogen diffusion and sulfide stress cracking of simulated heat-affected zone (HAZ) of A516- 65 grade steel were examined using an electrochemical permeation technique, glycerin volumetric method, and constant loading method. HAZ samples were fabricated using a metal thermal cycle simulator with a welding heat input of 20, 35, and 50.....
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Web of Science 4
Crossref 4
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스테인리스강 SS304의 균열 형상과 에치 피트를 이용한 응력부식균열 전파 기구 해석
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최병학, 이상우, 안종기, 이진희
Korean J. Met. Mater.
2020;58(9):583-589. Published online 2020 Aug 19
DOI:
https://doi.org/10.3365/KJMM.2020.58.9.583
Abstract
Austenitic stainless steel SS304 is vulnerable to Cl atmosphere SCC (stress corrosion crack). In this study, SCC phenomena related to stress and corrosion composition were analyzed to identify the mechanism for SCC initiation and propagation in SS304. The microstructure and mechanical properties resulting from crack propagation were analyzed by OM,.....
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Web of Science 2
Crossref 2
I
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Korean J. Met. Mater.
2019;57(10):663-672. Published online 2019 Sep 6
DOI:
https://doi.org/10.3365/KJMM.2019.57.10.663
Abstract
The dehydrogenation rates of graphene-added Mg (named Mg-5graphene) were very low at 573 K and 593 K. Ni was added to increase the dehydrogenation rates of graphene-added Mg. Samples (designated as Mg-2.5Ni-2.5graphene) with a composition of 95 wt% Mg + 2.5 wt% Ni + 2.5 wt% graphene were prepared by.....
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Web of Science 7
Crossref 6
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Korean J. Met. Mater.
2019;57(8):491-498. Published online 2019 Jul 11
DOI:
https://doi.org/10.3365/KJMM.2019.57.8.491
Abstract
Hydrogen-induced cracking (HIC) behavior was analyzed for gas metal arc (GMA) and laser beam (LB) welds on American Petroleum Institute (API) X65 steel. The GMA welds consisted of acicular ferrite (AF) with some widmanstatten ferrite (WF), while the LB welds had bainitic ferrite (BF) with some AF. The welds and.....
More
Web of Science 8
Crossref 7
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Korean J. Met. Mater.
2019;57(7):405-411. Published online 2019 Jun 5
DOI:
https://doi.org/10.3365/KJMM.2019.57.7.405
Abstract
This paper discusses a molybdenum-added alloy design for normalized pressure vessel steels, to reduce hydrogen induced cracking (HIC) and inhibit crack propagation. The change in microstructure produced by the modified alloy composition was analyzed to determine its effect on HIC characteristics. The microstructural change was observed by optical microscopy, hardness.....
More
Web of Science 5
Crossref 5
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Korean J. Met. Mater.
2019;57(6):390-395. Published online 2019 May 16
DOI:
https://doi.org/10.3365/KJMM.2019.57.6.390
Abstract
We demonstrate a synthetic route to high-quality Sn microcrystals using thermal chemical vapor deposition (CVD) in a hydrogen-reducing atmosphere. During thermal CVD with SnO2 powder, a mixture of Ar and H2 (4%) gases was used as a carrier gas to maintain a hydrogen reduction environment. Hydrogen maintained a reduction environment.....
More
Web of Science 2
Crossref 2
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Korean J. Met. Mater.
2019;57(4):245-250. Published online 2019 Apr 5
DOI:
https://doi.org/10.3365/KJMM.2019.57.4.245
Abstract
Copper leaching from low-grade copper ore samples obtained from two active mines in the US, named conichalcite (sample A) and chalcopyrite (sample B), were studied under different leaching conditions using sulfuric acid and methane sulfonic acid (MSA). The conichalcite, sample A, is calcium-copper arsenite hydroxide [CaCu(AsO4)(OH)] with small amount of.....
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Web of Science 4
Crossref 3
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Zr-2.5%Nb 압력관 재료에서 수소 농도와 균질화 처리 온도에 따른 수소화물 석출 거동
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임상엽, 김성수, 이경근
Korean J. Met. Mater.
2019;57(4):203-213. Published online 2019 Apr 5
DOI:
https://doi.org/10.3365/KJMM.2019.57.4.203
Abstract
The precipitation characteristics of hydrides in Zr-2.5% Nb pressure tube material were investigated for various hydrogen concentrations and homogenization temperatures. A surface hydride was formed using the electrolytic method and homogenized at various temperatures up to at 550 oC. The homogenization treatment was carried out at 300-550 oC over 240.....
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Web of Science 4
Crossref 3
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Korean J. Met. Mater.
2019;57(3):176-183. Published online 2019 Feb 8
DOI:
https://doi.org/10.3365/KJMM.2019.57.3.176
Abstract
In the present work, MgH2 was doped with Zn(BH4)2, Ni, and/or Ti to improve its hydrogen absorption and release features. Samples were prepared by grinding in a planetary ball mill in a hydrogen atmosphere. To increase the hydrogen absorption and release rates without significantly sacrificing hydrogenstorage capacity the additive percentages.....
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Web of Science 8
Crossref 7
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Korean J. Met. Mater.
2019;57(3):162-169. Published online 2019 Feb 8
DOI:
https://doi.org/10.3365/KJMM.2019.57.3.162
Abstract
During the extraction of metal ions from a weak acidic chloride solution by ionic liquids consisting of an organophosphorus extractant and Aliquat 336, the equilibrium pH is sometimes observed to be higher than the initial pH. To compare the hydrogen ion extraction behavior of tertiary and quaternary amines, Alamine 336,.....
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Web of Science 23
Crossref 21
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전기 방사를 이용한 1D / 2D 하이브리드 구조 고활성 MoS
2
/ CNF 수소 발생 촉매의 합성 및 특성 분석
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이정훈, 박유세, 장명제, 박성민, 이규환, 최우성, 최승목, 김양도
Korean J. Met. Mater.
2018;56(12):885-892. Published online 2018 Dec 5
DOI:
https://doi.org/10.3365/KJMM.2018.56.12.885
Abstract
Molybdenum disulfide (MoS2) based electrocatalysts have been proposed as substitutes for platinum group metal (PGM) based electrocatalyst to hydrogen evolution reaction (HER) in water electrolysis. Here, we studied MoS2/CNFs hybrid catalyst prepared by electrospinning method with heat treatment for polymer electrolyte membrane(PEM) water electrolysis to improve the HER activity. The.....
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Crossref 8
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Korean J. Met. Mater.
2018;56(12):878-884. Published online 2018 Dec 5
DOI:
https://doi.org/10.3365/KJMM.2018.56.12.878
Abstract
In the present work, we selected a polymer, polyvinylidene fluoride (PVDF), as an additive to improve the hydrogenation and dehydrogenation properties of Mg. 95 wt% Mg + 5 wt% PVDF (designated Mg-5PVDF) samples were prepared via milling in hydrogen atmosphere (reactive milling), and the hydrogenation and dehydrogenation characteristics of the.....
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Crossref 5
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Korean J. Met. Mater.
2018;56(11):829-834. Published online 2018 Nov 5
DOI:
https://doi.org/10.3365/KJMM.2018.56.11.829
Abstract
Although magnesium-based alloys are attractive materials for hydrogen storage applications, their activation properties, hydrogenation/dehydrogenation kinetics, thermodynamic equilibrium parameters, and degradation characteristics must be improved for practical applications. Further, magnesium poses several risks, including explosion hazard, environmental pollution, insufficient formability, and industrial damage. To overcome these problems, CaO-added Mg alloys, also.....
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